Table 2. Mass spectrometry data for diazepam, flunitrazepam and silylated temazepam as pure compounds and after extraction from beer as exemplar data.
Drug | Ion (m/z) | % intensity of pure compounds | % intensity after extraction from spiked beer |
Diazepam | 285 | 42 | 42 |
284 | 74 | 71 | |
283 | 97 | 94 | |
257 | 46 | 43 | |
256 | 100 | 100 | |
221 | 33 | 36 | |
Flunitrazepam | 313 | 67 | 69 |
312 | 100 | 100 | |
286 | 97 | 90 | |
266 | 61 | 59 | |
238 | 43 | 40 | |
183 | 20 | 20 | |
Silylated temazepam | 372 | 19 | 21 |
345 | 36 | 39 | |
344 | 25 | 26 | |
343 | 100 | 100 | |
283 | 31 | 37 | |
257 | 36 | 44 | |
221 | 6 | 7 |