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. Author manuscript; available in PMC: 2014 Feb 23.

Published in final edited form as: Nat Struct Mol Biol. 2012 Nov 11;19(12):1287–1292. doi: 10.1038/nsmb.2439

Table 1.

Data collection and refinement statistics (SAD)

	K₂PtCl₄ derivative
Data collection
Space group	P6122
Cell dimensions
a, b, c (Å)	72.10, 72.10, 323.55
α, β, γ (°)	90, 90, 120
Resolution (Å)	50–2.80 (2.90–2.80) ^*
R_sym or R_merge	0.083 (0.521)
I / σI	21.9 (1.9)
Completeness (%)	99.8 (99.1)
Redundancy	7.8 (8.1)
Refinement
Resolution (Å)	50–2.8
No. reflections
R_work / R_free	20.8/27.1
No. atoms
Protein	3040
Ligand/ion	13
Water	6
B-factors (Å²)	79.7
DAXX (main chain, side chain)	83.2, 87.9
H3.3 (main chain, side chain)	69.1, 73.6
H4 (main chain, side chain)	71.0, 75.2
Water	65.1
R.m.s. deviations
Bond lengths (Å)	0.006
Bond angles (°)	0.905

^*

Values in parentheses are for highest-resolution shell.