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. Author manuscript; available in PMC: 2014 Dec 11.
Published in final edited form as: J Am Chem Soc. 2013 Nov 22;135(49):18323–18326. doi: 10.1021/ja410478a

Table 2.

Scope of the Ketone-Enaminyl Radical Precursor.a

graphic file with name nihms544125t2.jpg
a

Reaction typically performed with 20 mol% of amine catalyst 3, 20 mol% of AcOH, 1 equiv. of LiAsF6, 2 equiv. of DABCO, 2 equiv. of water.

b

Reaction performed with 10 equiv. of water.

c

Diastereoselectivity determined by 1H NMR analysis.