Table 2.
1H-NMR and 13C-NMR data of compound 6.
| Atom no. | DEPT | δ H (mult., J in Hz) | δ C |
|---|---|---|---|
| 1 | C | 120.3 | |
| 2 | CH | 7.52 (1H, d, 1.9) | 112.7 |
| 3 | C | 147.5 | |
| 4 | C | 153.4 | |
| 5 | CH | 6.80 (1H, d, 8.0) | 115.4 |
| 6 | CH | 7.63 (1H, dd, 8.0, 1.9) | 125.6 |
| 7 | C | 166.7 | |
| 4-OCH3 | CH3 | 3.97 (3H, s) | 56.3 |
| 1′ | CH | 4.56 (1H, d, 7.2) | 98.3 |
| 2′ | CH | 3.39–3.62 (4H, m) | 73.4 |
| 3′ | CH | 78.7 | |
| 4′ | CH | 70.3 | |
| 5′ | CH | 74.5 | |
| 6′ | CH2 | 4.37 (1H, dd, 11.9, 2.0) 4.05 (1H, dd, 11.9, 7.4) |
64.2 |