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. 2014 Jan 21;70(Pt 2):173–181. doi: 10.1107/S2053230X14000144

Figure 3.

Figure 3

Conversion of 3-bromo-5-methoxyaniline to compound 3. a, 3-Bromo-5-methoxy­aniline, acetonitrile, heat and then 4-methylpiperidin-4-amine, DIPEA, microwave reaction; b, BBr3, dichloromethane.