Table 4. Unspecified impurity analysis of compounded 17-OHPC*.
| Sample | Impurity 1 % 17-OHPC | Impurity 2 % 17-OHPC | Impurity 3 % 17-OHPC | Total unspecified impurities % 17-OHPC |
|---|---|---|---|---|
| 1 | 0.03 | 0.16 | 0.05 | 0.24 |
| 2 | 0.11 | 0.14 | 0.04 | 0.29 |
| 3 | 0.08 | 0.01 | 0.06 | 0.15 |
| 4 | 0 | 0.04 | 0 | 0.04 |
| 5 | 0.01 | 0.30 | 0.04 | 0.35 |
| 6 | 0 | 0.20 | 0.02 | 0.22 |
| 7 | 0 | 0.07 | 0 | 0.07 |
| 8 | 0.04 | 0.03 | 0.01 | 0.08 |
| 9 | 0 | 0.05 | 0.02 | 0.07 |
| 10 | 0 | 0.06 | 0.02 | 0.08 |
| 11 | 0.02 | 0.20 | 0.01 | 0.23 |
| 12 | 0.04 | 0.03 | 0 | 0.07 |
| 13 | 0.07 | 0.10 | 0 | 0.17 |
| 14 | 0.07 | 0.08 | 0 | 0.15 |
| 15 | 0.20 | 0.05 | 0.03 | 0.28 |
| 16 | 0.02 | 0.16 | 0 | 0.18 |
| 17 | 0 | 0.07 | 0 | 0.07 |
| 18 | 0 | 0.07 | 0 | 0.07 |
| Mean ± SD | 0.04 ± 0.05 | 0.10 ± 0.08 | 0.02 ± 0.02 | 0.16 ± 0.09 |
| Median | 0.02 | 0.01 | 0.15 |
*
Quantification at wavelength of 242 nm
Impurity 1 – retention time 2.9 minutes Impurity
Impurity 2 – retention time 3.8 minutes Impurity
Impurity 3 – retention time 6.7 minutes