Table 1. Data collection and refinement statistics (Molecular replacement).
BCL6/Rifabutin | |
Data Collection | |
Space Group | P 1 21 1 |
Cell dimensions | |
a,b,c (Å) | 35.17, 54.83, 58.16 |
α,β,γ (°) | 90, 95.21, 90 |
Resolution (Å) | 39.82–2.3 (2.38–2.3) |
Rmerge | 10.8 (51.8) |
I/σI | 9.8 (4.1) |
Completeness (%) | 97.13 (97) |
Redundancy | 3.0 (2.9) |
Refinement | |
Resolution (Å) | 2.3 |
No. reflections | 9168 |
Rwork/Rfree | 20.2/26.9 |
No. Atoms | 2053 |
Protein | 1969 |
Ligand/ion | 61 |
Water | 23 |
B-factors | |
Protein | 27.9 |
Rifabutin | 48 |
Water | 24.6 |
R.M.S. deviations | |
Bond lengths (Å) | 0.013 |
Bond angles (°) | 1.885 |
*Highest resolution shell is shown in parenthesis.