Table 2. Summary of statistics and refinement of the BGLPf-M3 crystallographic data.
Values in parentheses are for the highest resolution shell.
| PDB entry | 3wdp |
| X-ray source | BL44XU, SPring-8 |
| Wavelength (Å) | 0.90 |
| Space group | C2 |
| Unit-cell parameters (Å, °) | a = 122.15, b = 161.15, c = 183.82, α = 90.00, β = 108.38, γ = 90.00 |
| Resolution range (Å) | 50.00–1.70 (1.76–1.70) |
| Total No. of reflections | 1214951 |
| No. of unique reflections | 367711 |
| Completeness (%) | 99.3 (99.1) |
| Mean I/σ(I) | 20.0 (3.9) |
| R merge † | 0.086 (0.361) |
| Refinement statistics | |
| Resolution range (Å) | 50.00–1.70 (1.76–1.70) |
| R factors‡ (R free/R work) | 0.233/0.212 (0.281/0.258) |
R
merge =
, where 〈I(hkl)〉 is the mean intensity of all reflections equivalent to reflection hkl.
R
work and R
free =
, where a randomly selected 5% of the data were used to calculate R
free.