Skip to main content
. 2014 Feb 19;2014:313609. doi: 10.1155/2014/313609

Table 2.

Assay results for the determination of IB and PA in their combined tablets.

% of label claim (mean ± SD, n = 6)
Method Alaxan Dibulaxan Febro
IB PA IB PA IB PA

HPLC 99.4 ± 0.9 99.8 ± 0.9 99.8 ± 1.3 99.4 ± 1.0 100.3 ± 1.0 99.3 ± 1.2

Derivative transform
1D spectra 99.5 ± 0.9 100.1 ± 1.4 100.3 ± 1.7 99.6 ± 1.3 99.4 ± 0.9 99.3 ± 1.3
1D ratio spectra 99.8 ± 1.3 99.1 ± 1.1 100.2 ± 1.5 99.3 ± 0.9 99.4 ± 1.5 100.1 ± 1.4

Wavelet transform
Sym6-spectra 100.3 ± 1.8 99.6 ± 1.3 100.3 ± 1.5 99.4 ± 1.2 100.6 ± 0.8 99.1 ± 1.0
Haar-spectra 99.3 ± 1.3 99.1 ± 1.2 100.3 ± 0.9 99.7 ± 1.7 100.5 ± 1.2 99.4 ± 0.9
Mexh-spectra 101.0 ± 1.2 100.7 ± 0.8 100.5 ± 1.8 98.8 ± 1.3 99.4 ± 0.9 99.6 ± 1.1
Sym6-ratio spectra 100.1 ± 1.1 99.1 ± 1.3 99.4 ± 0.9 100.4 ± 0.9 99.2 ± 1.1 99.8 ± 0.9
Haar-ratio spectra 99.7 ± 0.9 99.3 ± 0.6 100.1 ± 1.0 99.6 ± 1.1 100.6 ± 1.3 99.5 ± 1.1

Derivative-Wavelet transforms combined
Sym6-1D spectra 100.8 ± 1.4 100.0 ± 1.0 99.7 ± 1.2 101.0 ± 1.1 99.5 ± 1.4 100.5 ± 0.9
Haar-1D spectra 99.5 ± 0.8 99.5 ± 1.0 100.7 ± 1.1 100.9 ± 1.3 100.7 ± 0.8 99.8 ± 0.8
Mexh-1D spectra 99.7 ± 1.0 99.5 ± 0.9 99.8 ± 1.3 100.2 ± 1.5 99.7 ± 0.9 99.8 ± 1.2
1D-Sym6 spectra 100.5 ± 1.1 100.5 ± 0.8 99.8 ± 1.5 99.3 ± 1.4 100.6 ± 0.8 100.0 ± 1.1
1D-FWT spectra 99.9 ± 1.4 100.4 ± 1.3 100.1 ± 1.3 99.9 ± 1.2 100.4 ± 1.1 100.4 ± 1.0
Sym6-FWT spectra 100.7 ± 1.1 100.3 ± 0.9 100.4 ± 1.1 99.7 ± 1.4 99.6 ± 0.9 100.1 ± 0.9
Haar-FWT spectra 99.8 ± 1.3 99.9 ± 1.0 99.7 ± 1.5 100.1 ± 1.0 100.4 ± 1.2 100.6 ± 1.0
Mexh-FWT spectra 100.3 ± 0.9 99.6 ± 1.4 99.5 ± 1.6 100.7 ± 0.8 100.6 ± 0.8 99.7 ± 1.3