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Reactions performed under N2 atm; conversion (allylic phosphate consumption), site selectivities, and diastereoselectivities (±2%) were determined by analysis of 400 MHz 1H NMR spectra of product mixtures prior to purification; yields (±5%) are of products after purification; enantioselectivities (±2%) were determined by HPLC analysis. See the Supporting Information for experimental and analytical details.
