Table 2.
Design matrix and response values in Plackett–Burman factorial design for MAOS AS101 synthesis.
| X1a | X2a | X3a | X1b | X2b | X3b | Yield Method A | Yield Method B | |
|---|---|---|---|---|---|---|---|---|
| 1 | + | + | + | + | − | − | 73.5 ± 2.1 | 20.0 ± 4.2 |
| 2 | − | + | + | − | + | − | 78.5 ± 0.7 | 34.5 ± 2.1 |
| 3 | − | − | + | + | − | + | 67.0 ± 2.8 | 38.0 ± 5.7 |
| 4 | + | − | − | + | + | − | 53.0 ± 1.4 | 45.0 ± 0.3 |
| 5 | − | + | − | + | + | + | 78.5 ± 0.7 | 36.5 ± 0.7 |
| 6 | + | − | + | − | + | + | 75.5 ± 0.7 | 31.0 ± 2.8 |
| 7 | + | + | − | − | − | + | 53.0 ± 1.4 | 33.0 ± 1.4 |
| 8 | − | − | − | − | − | − | 0 | 0 |
Method A: X1a (power), X2a (pressure) and X3a (time); Method B: X1b (power), X2b (temperature) and X3b (time).