Table 1. Scope of the Intramolecular Reductive Coupling.
a
Used 30 mol% Fe(acac)3 in EtOH/(CH2OH)2 (5:1).
b
Used 20 mol% Fe(acac)3 in DCE/(CH2OH)2 (5:1).
c
Run on gram-scale with 2.0 equiv PhSiH3.
d
Used 1.5 equiv PhSiH3.
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