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. 2014 Feb 20;289(14):10104–10114. doi: 10.1074/jbc.M113.519298

TABLE 1.

1H and 13C chemical shifts of U1 identified as 1,2-diacyl-3-α-d-Glcp-sn-Gro reported (internal standard, tetramethylsilane)

Spectra were recorded in CDCl3 at 27 °C utilizing a Bruker DRX Avance 700 spectrometer. Gro stands for glycerol.

1a 1b 2 3a 3b 4 5 6a 6b
α-d-Glcp
    H (δ) 4.85 (3J1,2 2.6 Hz) 3.50 3.72 3.58 3.59 3.81 3.83
    C (δ) 99.13 72.16 74.30 70.05 71.85 61.84

Gro
    H (δ) 4.39 4.15 5.24 3.81 3.60
    C (δ) 62.41 69.85 66.35