Table 1. List of HDL Glycans with Retention Times, Their m/z Values, Charge States, Glycan Compositions, and the Ion Intensities.
retention time (min) | measured m/z | charge state | mass error (ppm) | hexose | HexNAc | fucose | NeuAc | ion intensity (counts) |
---|---|---|---|---|---|---|---|---|
24.839 | 1112.403 | 2 | 3.57 | 5 | 4 | 0 | 2 | 6091078 |
23.541 | 1112.402 | 2 | 2.94 | 5 | 4 | 0 | 2 | 4906932 |
19.915 | 966.8551 | 2 | 4.13 | 5 | 4 | 0 | 1 | 1196125 |
18.466 | 966.8576 | 2 | 6.78 | 5 | 4 | 0 | 1 | 797081 |
22.675 | 966.8543 | 2 | 3.37 | 5 | 4 | 0 | 1 | 129647 |
17.355 | 966.8556 | 2 | 4.65 | 5 | 4 | 0 | 1 | 78041 |
17.725 | 865.3141 | 2 | 3.12 | 5 | 3 | 0 | 1 | 171480 |
16.31 | 865.3134 | 2 | 2.38 | 5 | 3 | 0 | 1 | 47271 |
24.524 | 1039.883 | 2 | 2.91 | 5 | 4 | 1 | 1 | 141126 |
22.706 | 1039.883 | 2 | 2.99 | 5 | 4 | 1 | 1 | 95666 |
23.434 | 1039.884 | 2 | 3.92 | 5 | 4 | 1 | 1 | 41850 |
20.862 | 1039.878 | 2 | –1.68 | 5 | 4 | 1 | 1 | 19297 |
17.857 | 894.3368 | 2 | 4.97 | 5 | 4 | 1 | 0 | 140215 |
16.374 | 894.3332 | 2 | 0.98 | 5 | 4 | 1 | 0 | 58633 |
15.169 | 821.3112 | 2 | 9.56 | 5 | 4 | 0 | 0 | 93233 |
13.997 | 821.3069 | 2 | 4.31 | 5 | 4 | 0 | 0 | 43677 |
25.483 | 1185.427 | 2 | –0.37 | 5 | 4 | 1 | 2 | 62932 |
19.253 | 784.2855 | 2 | 0.65 | 4 | 3 | 0 | 1 | 55095 |
16.874 | 813.3067 | 2 | 0.92 | 4 | 4 | 1 | 0 | 53118 |
19.206 | 885.8271 | 2 | 2.78 | 4 | 4 | 0 | 1 | 48338 |
17.746 | 885.8248 | 2 | 0.15 | 4 | 4 | 0 | 1 | 24690 |
12.726 | 942.3367 | 2 | 7.5 | 9 | 2 | 0 | 0 | 38575 |
11.579 | 942.3349 | 2 | 5.58 | 9 | 2 | 0 | 0 | 16327 |
23.563 | 1258.465 | 2 | 6.4 | 5 | 4 | 2 | 2 | 37927 |
21.401 | 1076.901 | 2 | 2.33 | 6 | 5 | 1 | 0 | 30048 |
24.534 | 1294.957 | 2 | –5.19 | 6 | 5 | 0 | 2 | 25651 |
16.092 | 732.2802 | 2 | 0.95 | 3 | 4 | 1 | 0 | 22085 |