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. 2014 Mar 25;70(Pt 4):464–466. doi: 10.1107/S2053230X14001940

Table 1. Statistics of data collection and refinement.

Values in parentheses are for the outermost resolution shell.

Beamline BL-5A, PF
Detector ADSC Quantum 315r
Crystal-to-detector distance (mm) 249.6
Wavelength (Å) 1.0000
No. of images 600
Oscillation range (°) 0–180
Resolution range (Å) 50.0–2.15 (2.28–2.15)
No. of total reflections 518379 (82634)
No. of unique reflections 71192 (11231)
Space group P212121
Unit-cell parameters (Å) a = 60.2, b = 119.2, c = 177.2
Completeness (%) 99.7 (98.7)
R meas (%) 8.9 (52.6)
I/σ(I)〉 20.81 (5.75)
Crystal mosaicity (°) 0.15
Wilson B factor (Å2) 35.27