Table 1. Data-collection statistics of CbHBD.
Beamline | 7A, PAL |
Wavelength (Å) | 1.0 |
Temperature (K) | 100 |
Oscillation (°) | 1.0 |
Mosaicity (°) | 0.81 |
Total rotation range (°) | 180 |
Space group | R3 |
Unit-cell parameters (Å, °) | a = b = 148.5, c = 201.6, α = β = 90.0, γ = 120.0 |
Resolution (Å) | 50.0–2.30 (2.38–2.30) |
Total reflections | 243475 |
Unique reflections | 65804 |
Completeness (%) | 93.5 (89.6) |
R merge † (%) | 6.6 (29.6) |
〈I/σ(I)〉 | 29.9 (2.9) |
Multiplicity | 3.7 (3.1) |
R merge = , where I i(hkl) and 〈I(hkl)〉 are the observed individual and mean intensities of a reflection, respectively. is the sum over the individual measurements of a reflection and is the sum over all reflections.