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. 2014 Mar 25;70(Pt 4):489–492. doi: 10.1107/S2053230X14004543

Table 1. Data collection statistics for vvMTase.

Values in parentheses are for the highest resolution shell.

Synchrotron 5C SBII, PAL
Wavelength (Å) 0.98
Space group P21
Unit-cell parameters (Å, °) a = 93.25, b = 133.04, c = 121.49, α = γ = 90, β = 109.7
Resolution range (Å) 50–2.31 (2.37–2.31)
Completeness (%) 91.7 (83.9)
R merge (%) 13.4 (30.9)
Measured reflections 284629
Unique reflections 110965
Multiplicity 2.6 (2.0)
Temperature (K) 100
Matthews coefficient (Å3 Da−1) 2.61
Solvent content (%) 53
No. of molecules in asymmetric unit 4
Mean I/σ(I) 9.67 (2.37)

R merge = Inline graphic Inline graphic, where Ii(hkl) is the observed intensity of an individual reflection and 〈I(hkl)〉 is the mean intensity of that reflection.