Table 1. Data-collection and processing statistics.
Values in parentheses are for the highest resolution shell.
| Crystal improved by streak-seeding | Crystal improved with Triton X-114 | |
|---|---|---|
| ESRF beamline | ID14-1 | ID23 |
| Strategy | 180°, Δϕ 0.5° | 180°, Δϕ 0.5° |
| Wavelength | 0.9334 | 0.9801 |
| Space group | P21 | P212121 |
| Unit-cell parameters | ||
| a (Å) | 55.98 | 52.56 |
| b (Å) | 131.19 | 57.57 |
| c (Å) | 56.71 | 128.72 |
| α (°) | 90.0 | 90.0 |
| β (°) | 91.1 | 90.0 |
| γ (°) | 90.0 | 90.0 |
| Resolution limits (Å) | 42.97–2.22 (2.34–2.22) | 27.46–2.30 (2.42–2.30) |
| Solvent content (%) | 45.6 | 45.0 |
| Molecules in the asymmetric unit | 4 | 2 |
| R merge | 0.08 (0.47) | 0.16 (0.59) |
| Mean I/σ(I) | 12.2 (2.6) | 7.9 (3.0) |