Table 1. Data collection and refinement statistics.
aεFab1–IgE-Fc–aεFab2 | |
---|---|
Data collection | |
Space group | P2l2121 |
Cell dimensions | |
a, b, c (Α̊) | 84.59, 100.81, 219.68 |
α, β, γ (°) | 90.0, 90.0, 90.0 |
Resolution (Α̊) | 2.91 (2.98 – 2.91)* |
R merge | 0.055 (0.796) |
I / σI | 18.4 (3.0) |
Completeness (%) | 99.7 (99.2) |
Redundancy | 5.7 (6.0) |
Refinement | |
Resolution (Α̊) | 67.01 – 2.91 |
No. unique reflections | 41987 (3078) |
Rwork / Rfree | 0.236 / 0.284 |
No. atoms | 11712 |
Protein | 11541 |
Ligand/ion | 122 |
Water | 49 |
β factors | |
Protein | 103.8 |
Ligand/ion | 110.9a |
Water | 88.4 |
r.m.s. deviations | |
Bond lengths (Α̊) | 0.010 |
Bond angles (°) | 1.566 |
Values in parentheses are for highest-resolution shell.