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Partial 1H NMR (600 MHz, CDCl3, 300 K), with selected signals assigned, of (i) macrocycle 2, (ii) (d,Rmp)-4, (iii) (d,Smp)-4, and (iv) their corresponding non-interlocked thread. See the Supporting Information for full assignment. Labeling is as shown in Scheme 1. Residual solvent signals are shown in gray.
