Table 2.
Crystallization, data collection and refinement parameters for the PO4-complexed and GMP-complexed crystal forms of LpcN-II.
| PO4-complexed LpcN-II | GMP-complexed LpcN-II | |
|---|---|---|
| Resolution | 20-2.70 | 44.70-2.53 |
| No. of reflections | 29199 | 71361 |
| No. of reflections for Rfree | 2920 | 6753 |
| Rvalue | 0.222 | 0.231 |
| Rfree | 0.258 | 0.272 |
| RMS deviation-Bond length | 0.007 | 0.007 |
| RMS deviation-Bond angle | 1.4 | 1.4 |
| Mean B-value (overall) | 61.7 | 54.3 |
| B-value from Wilson plot | 60.1 | 60.2 |
| % residues (most favourable) | 90.6 | 89.9 |
| % residues (additionally allowed) | 8.0 | 9.2 |
| % residues (generously allowed) | 1.4 | 0.9 |
| % residues (disallowed) | 0.0 | 0.0 |
| PDB ID | 4G63 | 4OHF |