Table 1. Quality Assurance and Quality Control Data for Analysis of Tissue Samples.
| sample | element | LODa[μg/g (ppmb)] | blank | duplicate RPDc (%) | LCS,d % recovery | spike, % recovery | SRM,e % recovery |
|---|---|---|---|---|---|---|---|
| tissue | Cr | 0.10 | BDLf | 8.6 | 103.4 | 95.9 | 111.4 |
| tissue | Ni | 0.09 | BDL | 8.5 | 102.0 | 95.5 | 70.3 |
| tar ball | Cr | 0.67 | BDL | g | 91.6 | 94.3 | nah |
| tar ball | Ni | 0.22 | BDL | 4.7 | 92.1 | 91.4 | na |
| oil slick | Cr | 0.57 | BDL | g | 100.8 | 100.1 | na |
| oil slick | Ni | 0.57 | BDL | 5.7 | 99.5 | 97.5 | na |
LOD = limit of detection.
ppm = parts per million.
RPD = relative percent difference.
LCS = laboratory control sample.
SRM = standard reference material (DOLT-4; DORM-3).
BDL = below detection limit.
All duplicate measurements were below the project quantitation limit.
na = not applicable.