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X-band EPR spectra of 400 μM CuDHX1 in CH3OH. Top: CuDHX1 before (black line) and after addition of 5000 equiv of NO (red line). Middle: CuDHX1 before (black line) and after (red line) addition of 100 equiv of Angeli’s salt. Bottom: CuDHX1 after reduction by HNO (black line) and after reoxidation by air (red line). Collection parameters: temperature, 77 K; modulation amplitude, 20 G; microwave power, 0.2 mW at 9.23 GHz.
