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. Author manuscript; available in PMC: 2014 Apr 14.
Published in final edited form as: Inorg Chem. 2007 Sep 29;46(22):9285–9293. doi: 10.1021/ic7012667

Figure 3.

Figure 3

Bottom: 51V SSNMR spectrum of 1 acquired at 9.4 T with an MAS rate of 11 kHz. The inset spectrum is an expansion of the central transition region of the spectrum illustrating the lack of second-order quadrupolar lineshapes. Top: a stationary spectrum calculated using the parameters in table 1 illustrating the contributions from the central transition (dark grey) and the satellite transitions (light grey). The spinning side band envelope in the experimental spectrum mimics the overall lineshape of these calculated spectra.