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. 2010 Apr 30;2(2):159–170. doi: 10.3390/pharmaceutics2020159

Table 2.

Inter-day accuracy and precision of the LLOQ, LQC, MQC, HQC, and ULOQ evaluation samples for the dog whole blood method. Mean values in the table are the average of the back-calculated concentrations from the standard curve.

QC sample (ng/mL) Compound A Metabolite
LLOQ LQC MQC HQC ULOQ LLOQ LQC MQC HQC ULOQ
10.8 22.1 276 2,300 2,730 3.17 6.72 84.0 700 811
n 18 18 18 18 18 18 18 18 18 18
Mean 11.5 22.9 290 2,350 2,680 3.36 6.98 84.9 721 835
CV (%) 4.7 5.0 2.5 4.8 5.0 14.5 8.0 3.3 4.4 4.0
Bias (%) 6.5 3.6 5.1 2.2 -1.8 6.0 3.9 1.1 3.0 3.0