Table 1.
Data collection and refinement statistics
| OspG/UbcH5c-O∼Ub | |
|---|---|
| Data collection | |
| Space group | P6322 |
| Cell dimensions | |
| a,b,c (Å) | 183.87, 183.87, 63.97 |
| α, β, γ (°) | 90, 90, 120 |
| Resolution (Å) | 50–2.70 (2.80–2.70)a |
| Rsym | 0.202 (1.0) |
| I/σI | 16.39 (2.58) |
| Completeness (%) | 99.97 (99.83) |
| Redundancy | 19.1 (11.2) |
| Refinement | |
| Resolution (Å) | 44.16–2.70 |
| No. reflections | 17947 |
| Rwork/Rfree | 0.244/0.291 |
| No. atoms | 3226 |
| Protein | 3165 |
| Ligand/ion | 0 |
| Water | 61 |
| B-factors | |
| Protein | 22.20 |
| Water | 14.10 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.005 |
| Bond angles (°) | 0.92 |
| Ramanchandran statistics | |
| No. of non-glycine/proline residues | 344 |
| Residues in most favored regions | 91.3% |
| Residues in additionally allowed regions | 8.4% |
| Residues in generously allowed regions | 0.0% |
| Residues in disallowed regions | 0.3% |
a
Values in parentheses are for highest-resolution shell.