TABLE 1.
MRM monitoring mass spectrometer conditions
Analyte | Mode | Q1 mass (m/z) | Q3 mass (m/z) | Dwell time (ms) | DP (V) | CE (V) | CXP (V) | EP (V) | IS (V) | Temp (°C) | GS1 | GS2 |
---|---|---|---|---|---|---|---|---|---|---|---|---|
ATV | + | 705.4 | 168.2 | 100 | 120.0 | 101.0 | 13.0 | 10.0 | 5,500 | 450 | 80 | 70 |
ATV-IS | + | 711.5 | 168.1 | 100 | 120.0 | 101.0 | 13.0 | 10.0 | 5,500 | 450 | 80 | 70 |
DRV | + | 548.3 | 392.3 | 100 | 100.0 | 18.5 | 16.0 | 10.0 | 5,500 | 450 | 80 | 70 |
EFV | − | 313.9 | 244.0 | 300 | −30.0 | −22.0 | −16.0 | −10.0 | −4,500 | 650 | 50 | 90 |
EFV-IS | − | 322.0 | 251.1 | 300 | −30.0 | −22.0 | −16.0 | −10.0 | −4,500 | 650 | 50 | 90 |
LPV | + | 629.4 | 447.3 | 100 | 84.0 | 19.5 | 12.0 | 10.0 | 5,500 | 450 | 80 | 70 |
RTV | + | 721.4 | 268.2 | 100 | 95.0 | 37.0 | 14.0 | 10.0 | 5,500 | 450 | 80 | 70 |
RTV-IS | + | 729.4 | 276.3 | 100 | 95.0 | 37.0 | 14.0 | 10.0 | 5,500 | 450 | 80 | 70 |