Skip to main content
. 2014 Feb 17;77(2):227–233. doi: 10.1021/np4006635

Table 2. 13C NMR Data (100 MHz, in CD3OD) of 15 and 8, δ in ppm.

no. 1 2a 2aa 3 4 5 8
2 152.7, CH 153.2, CH 153.5, CH 152.8, CH 152.8, CH 152.6, CH 152.7, CH
4 149.2, C 149.5, C 149.7, C 149.1, C 149.1, C 148.9, C 149.1, C
5 118.3, C 118.8, C 118.5, C 118.0, C 118.1, C 118.0, C 118.0, C
6 156.0, C 156.5, C 156.5, C 155.9, C 156.0, C 155.8, C 156.0, C
8 139.2, CH 140.7, CH 138.9, CH 139.0, CH 139.5, CH 141.0, CH 139.5, CH
1′ 89.6, CH 87.2, CH 86.8, CH 88.0, CH 87.1, CH 87.7, CH 87.3, CH
2′ 81.0, CH 90.8, CH 89.7, CH 89.5, CH 90.3, CH 90.8, CH 90.3, CH
3′ 76.4, CH 73.0, CH 72.7, CH 72.5, CH 73.1, CH 72.4, CH 73.2, CH
4′ 77.5, CH 77.8, CH 77.5, CH 78.4, CH 77.7, CH 78.3, CH 77.5, CH
5′ 25.3, CH2 26.4, CH2 25.5, CH2 25.0, CH2 25.1, CH2 25.0, CH2 25.2, CH2
6′ 65.2, CH 66.3, CH 57.9, CH 69.6, CH 65.1, CH 64.1, CH 65.2, CH
7′ 91.8, C 94.5, C 94.1, C 94.2, C 92.0, C 93.3, C 91.9, C
8′ 70.5, CH 92.6, C 200.5, C 68.4, CH 70.5, CH 69.9, CH 70.5, CH
9′ 69.0, CH 38.4, CH2 40.6, CH2 70.7, CH 69.2, CH 73.0, CH 69.1, CH
10′ 76.9, CH 71.0, CH 74.6, CH 79.0, CH 76.9, CH 76.6, CH 76.9, CH
11′ 169.8, C 172.3, C 170.9, C 169.9, C 170.0, C 170.4, C 169.8, C
1″ 165.8, C       164.7, C   165.7, C
2″ 129.6, C       131.1, C   127.0, C
3″ 140.4, CH       144.3, CH   140.3, CH
4″ 13.6, CH3       13.7, CH3   13.7, CH3
5″ 10.9, CH3       54.9, CH2   10.9, CH3
2′-OCH3   57.9 58.0 57.1 56.9 57.0 56.9
11′-OCH3 51.3 51.7 52.7 51.4 51.4 50.9 51.3
a

Measured in DMSO-d6.