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. 2014 Feb 19;70(Pt 3):o318–o319. doi: 10.1107/S1600536814003146
O1B—C1B 1.2803 (18) N1A—C2A 1.375 (2)
O2B—H2B 0.8400 N2A—C1A 1.3472 (19)
O2B—C7B 1.3019 (18) N2A—C3A 1.3748 (19)
O3B—C7B 1.2249 (18) N2A—C4A 1.4660 (19)
O4B—N2B 1.2303 (18) N3A—H3AA 0.9100
O5B—N2B 1.2261 (18) N3A—H3AB 0.9100
O6B—N1B 1.2300 (18) N3A—H3AC 0.9100
O7B—N1B 1.2224 (18) N3A—C6A 1.4844 (19)
N1B—C6B 1.4629 (19) C1A—H1A 0.9500
N2B—C4B 1.4540 (18) C2A—H2A 0.9500
C1B—C2B 1.441 (2) C2A—C3A 1.352 (2)
C1B—C6B 1.433 (2) C3A—H3A 0.9500
C2B—C3B 1.373 (2) C4A—H4AA 0.9900
C2B—C7B 1.498 (2) C4A—H4AB 0.9900
C3B—H3B 0.9500 C4A—C5A 1.517 (2)
C3B—C4B 1.385 (2) C5A—H5AA 0.9900
C4B—C5B 1.381 (2) C5A—H5AB 0.9900
C5B—H5B 0.9500 C5A—C6A 1.510 (2)
C5B—C6B 1.377 (2) C6A—H6AA 0.9900
N1A—C1A 1.320 (2) C6A—H6AB 0.9900
C7B—O2B—H2B 109.5 H3AA—N3A—H3AC 109.5
O6B—N1B—C6B 117.54 (13) H3AB—N3A—H3AC 109.5
O7B—N1B—O6B 123.30 (14) C6A—N3A—H3AA 109.5
O7B—N1B—C6B 119.17 (13) C6A—N3A—H3AB 109.5
O4B—N2B—C4B 118.05 (13) C6A—N3A—H3AC 109.5
O5B—N2B—O4B 123.43 (13) N1A—C1A—N2A 111.69 (13)
O5B—N2B—C4B 118.52 (13) N1A—C1A—H1A 124.2
O1B—C1B—C2B 120.31 (13) N2A—C1A—H1A 124.2
O1B—C1B—C6B 124.78 (14) N1A—C2A—H2A 124.8
C6B—C1B—C2B 114.84 (13) C3A—C2A—N1A 110.33 (14)
C1B—C2B—C7B 119.59 (13) C3A—C2A—H2A 124.8
C3B—C2B—C1B 121.69 (14) N2A—C3A—H3A 127.0
C3B—C2B—C7B 118.70 (13) C2A—C3A—N2A 105.94 (14)
C2B—C3B—H3B 120.0 C2A—C3A—H3A 127.0
C2B—C3B—C4B 120.03 (14) N2A—C4A—H4AA 109.1
C4B—C3B—H3B 120.0 N2A—C4A—H4AB 109.1
C3B—C4B—N2B 119.02 (13) N2A—C4A—C5A 112.48 (12)
C5B—C4B—N2B 119.37 (13) H4AA—C4A—H4AB 107.8
C5B—C4B—C3B 121.60 (13) C5A—C4A—H4AA 109.1
C4B—C5B—H5B 120.7 C5A—C4A—H4AB 109.1
C6B—C5B—C4B 118.69 (14) C4A—C5A—H5AA 109.3
C6B—C5B—H5B 120.7 C4A—C5A—H5AB 109.3
C1B—C6B—N1B 120.14 (13) H5AA—C5A—H5AB 108.0
C5B—C6B—N1B 116.69 (13) C6A—C5A—C4A 111.50 (12)
C5B—C6B—C1B 123.12 (14) C6A—C5A—H5AA 109.3
O2B—C7B—C2B 116.03 (13) C6A—C5A—H5AB 109.3
O3B—C7B—O2B 121.99 (14) N3A—C6A—C5A 112.37 (12)
O3B—C7B—C2B 121.96 (13) N3A—C6A—H6AA 109.1
C1A—N1A—C2A 105.07 (13) N3A—C6A—H6AB 109.1
C1A—N2A—C3A 106.97 (13) C5A—C6A—H6AA 109.1
C1A—N2A—C4A 125.58 (13) C5A—C6A—H6AB 109.1
C3A—N2A—C4A 127.43 (13) H6AA—C6A—H6AB 107.9
H3AA—N3A—H3AB 109.5
O1B—C1B—C2B—C3B −178.23 (13) C3B—C2B—C7B—O2B 179.26 (13)
O1B—C1B—C2B—C7B 0.3 (2) C3B—C2B—C7B—O3B 1.0 (2)
O1B—C1B—C6B—N1B −0.9 (2) C3B—C4B—C5B—C6B −0.6 (2)
O1B—C1B—C6B—C5B 176.43 (14) C4B—C5B—C6B—N1B 178.87 (13)
O4B—N2B—C4B—C3B 3.8 (2) C4B—C5B—C6B—C1B 1.5 (2)
O4B—N2B—C4B—C5B −177.14 (13) C6B—C1B—C2B—C3B −0.9 (2)
O5B—N2B—C4B—C3B −176.02 (14) C6B—C1B—C2B—C7B 177.58 (12)
O5B—N2B—C4B—C5B 3.0 (2) C7B—C2B—C3B—C4B −176.73 (13)
O6B—N1B—C6B—C1B 154.04 (15) N1A—C2A—C3A—N2A 0.13 (18)
O6B—N1B—C6B—C5B −23.4 (2) N2A—C4A—C5A—C6A −69.71 (16)
O7B—N1B—C6B—C1B −25.8 (2) C1A—N1A—C2A—C3A 0.02 (18)
O7B—N1B—C6B—C5B 156.73 (14) C1A—N2A—C3A—C2A −0.23 (17)
N2B—C4B—C5B—C6B −179.60 (13) C1A—N2A—C4A—C5A −80.85 (18)
C1B—C2B—C3B—C4B 1.8 (2) C2A—N1A—C1A—N2A −0.17 (18)
C1B—C2B—C7B—O2B 0.7 (2) C3A—N2A—C1A—N1A 0.26 (18)
C1B—C2B—C7B—O3B −177.60 (13) C3A—N2A—C4A—C5A 97.42 (17)
C2B—C1B—C6B—N1B −178.03 (12) C4A—N2A—C1A—N1A 178.83 (13)
C2B—C1B—C6B—C5B −0.7 (2) C4A—N2A—C3A—C2A −178.77 (14)
C2B—C3B—C4B—N2B 177.99 (13) C4A—C5A—C6A—N3A 175.16 (12)
C2B—C3B—C4B—C5B −1.0 (2)