| Agilent Xcalibur (Eos, Gemini) diffractometer | 2953 independent reflections |
| Radiation source: Enhance (Cu) X-ray Source | 2582 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.026 |
| Detector resolution: 16.0416 pixels mm-1 | θmax = 72.5°, θmin = 4.2° |
| ω scans | h = −8→5 |
| Absorption correction: multi-scan (CrysAlis PRO and CrysAlis RED; Agilent, 2012) | k = −12→13 |
| Tmin = 0.925, Tmax = 1.000 | l = −13→13 |
| 4664 measured reflections |
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