| Bruker SMART APEX CCD diffractometer | 2042 independent reflections |
| Radiation source: fine-focus sealed tube | 1567 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.025 |
| ω scan | θmax = 25.5°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Bruker, 2000) | h = −7→7 |
| Tmin = 0.954, Tmax = 0.994 | k = −10→10 |
| 6541 measured reflections | l = −23→24 |
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