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. 2014 Feb 12;70(Pt 3):o288. doi: 10.1107/S1600536814001986
Bruker SMART APEXII CCD diffractometer 4956 independent reflections
Radiation source: fine-focus sealed tube 3416 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.048
φ and ω scans θmax = 30.6°, θmin = 2.0°
Absorption correction: multi-scan (SADABS; Bruker, 2009) h = −23→23
Tmin = 0.868, Tmax = 0.972 k = −7→7
16728 measured reflections l = −25→29