Bruker SMART APEXII CCD diffractometer | 4956 independent reflections |
Radiation source: fine-focus sealed tube | 3416 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.048 |
φ and ω scans | θmax = 30.6°, θmin = 2.0° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −23→23 |
Tmin = 0.868, Tmax = 0.972 | k = −7→7 |
16728 measured reflections | l = −25→29 |