N1—C9 | 1.351 (5) | C15—H15A | 0.9900 |
N1—C2 | 1.381 (5) | C15—H15B | 0.9900 |
N1—H1 | 0.8800 | C16—C17 | 1.524 (6) |
C2—C3 | 1.356 (6) | C16—H16A | 0.9900 |
C2—H2 | 0.9500 | C16—H16B | 0.9900 |
C3—C4 | 1.452 (6) | C17—C18 | 1.519 (6) |
C3—H3 | 0.9500 | C17—H17 | 1.0000 |
C4—C9 | 1.378 (5) | C18—H18A | 0.9800 |
C4—C5 | 1.410 (6) | C18—H18B | 0.9800 |
C5—N10 | 1.352 (5) | C18—H18C | 0.9800 |
C5—N6 | 1.359 (5) | C19—C20 | 1.523 (6) |
N6—C7 | 1.323 (5) | C19—C23 | 1.534 (6) |
C7—N8 | 1.312 (5) | C19—C22 | 1.538 (6) |
C7—H7 | 0.9500 | C20—O21 | 1.458 (5) |
N8—C9 | 1.369 (6) | C20—H20A | 0.9900 |
N10—C12 | 1.467 (5) | C20—H20B | 0.9900 |
N10—C11 | 1.476 (5) | O21—C22 | 1.456 (6) |
C11—H11A | 0.9800 | C22—H22A | 0.9900 |
C11—H11B | 0.9800 | C22—H22B | 0.9900 |
C11—H11C | 0.9800 | C23—C24 | 1.459 (7) |
C12—C13 | 1.521 (6) | C23—H23A | 0.9900 |
C12—C17 | 1.538 (6) | C23—H23B | 0.9900 |
C12—H12 | 1.0000 | C24—N25 | 1.145 (6) |
C13—N14 | 1.463 (5) | O1L—H1L1 | 1.0100 |
C13—H13A | 0.9900 | O1L—H1L2 | 0.8390 |
C13—H13B | 0.9900 | O1L—H2L1 | 1.0319 |
N14—C19 | 1.445 (5) | O2L—H1L1 | 0.3669 |
N14—C15 | 1.458 (5) | O2L—H2L1 | 0.8478 |
C15—C16 | 1.520 (6) | O2L—H2L2 | 0.8441 |
C9—N1—C2 | 108.3 (3) | H15A—C15—H15B | 108.3 |
C9—N1—H1 | 125.8 | C15—C16—C17 | 112.0 (4) |
C2—N1—H1 | 125.8 | C15—C16—H16A | 109.2 |
C3—C2—N1 | 109.2 (4) | C17—C16—H16A | 109.2 |
C3—C2—H2 | 125.4 | C15—C16—H16B | 109.2 |
N1—C2—H2 | 125.4 | C17—C16—H16B | 109.2 |
C2—C3—C4 | 107.1 (4) | H16A—C16—H16B | 107.9 |
C2—C3—H3 | 126.4 | C18—C17—C16 | 111.0 (4) |
C4—C3—H3 | 126.4 | C18—C17—C12 | 112.2 (3) |
C9—C4—C5 | 115.8 (4) | C16—C17—C12 | 112.6 (4) |
C9—C4—C3 | 105.3 (4) | C18—C17—H17 | 106.9 |
C5—C4—C3 | 138.7 (4) | C16—C17—H17 | 106.9 |
N10—C5—N6 | 116.0 (4) | C12—C17—H17 | 106.9 |
N10—C5—C4 | 125.3 (4) | C17—C18—H18A | 109.5 |
N6—C5—C4 | 118.6 (4) | C17—C18—H18B | 109.5 |
C7—N6—C5 | 118.1 (4) | H18A—C18—H18B | 109.5 |
N8—C7—N6 | 130.0 (4) | C17—C18—H18C | 109.5 |
N8—C7—H7 | 115.0 | H18A—C18—H18C | 109.5 |
N6—C7—H7 | 115.0 | H18B—C18—H18C | 109.5 |
C7—N8—C9 | 110.8 (4) | N14—C19—C20 | 113.7 (3) |
N1—C9—N8 | 123.3 (4) | N14—C19—C23 | 114.2 (4) |
N1—C9—C4 | 110.1 (4) | C20—C19—C23 | 113.3 (4) |
N8—C9—C4 | 126.5 (4) | N14—C19—C22 | 113.6 (4) |
C5—N10—C12 | 121.8 (3) | C20—C19—C22 | 85.2 (3) |
C5—N10—C11 | 118.8 (3) | C23—C19—C22 | 113.6 (3) |
C12—N10—C11 | 119.4 (3) | O21—C20—C19 | 91.4 (3) |
N10—C11—H11A | 109.5 | O21—C20—H20A | 113.4 |
N10—C11—H11B | 109.5 | C19—C20—H20A | 113.4 |
H11A—C11—H11B | 109.5 | O21—C20—H20B | 113.4 |
N10—C11—H11C | 109.5 | C19—C20—H20B | 113.4 |
H11A—C11—H11C | 109.5 | H20A—C20—H20B | 110.7 |
H11B—C11—H11C | 109.5 | C22—O21—C20 | 90.6 (3) |
N10—C12—C13 | 114.1 (3) | O21—C22—C19 | 90.9 (3) |
N10—C12—C17 | 114.3 (3) | O21—C22—H22A | 113.5 |
C13—C12—C17 | 110.9 (3) | C19—C22—H22A | 113.5 |
N10—C12—H12 | 105.5 | O21—C22—H22B | 113.5 |
C13—C12—H12 | 105.5 | C19—C22—H22B | 113.5 |
C17—C12—H12 | 105.5 | H22A—C22—H22B | 110.8 |
N14—C13—C12 | 112.9 (4) | C24—C23—C19 | 112.2 (4) |
N14—C13—H13A | 109.0 | C24—C23—H23A | 109.2 |
C12—C13—H13A | 109.0 | C19—C23—H23A | 109.2 |
N14—C13—H13B | 109.0 | C24—C23—H23B | 109.2 |
C12—C13—H13B | 109.0 | C19—C23—H23B | 109.2 |
H13A—C13—H13B | 107.8 | H23A—C23—H23B | 107.9 |
C19—N14—C15 | 114.1 (3) | N25—C24—C23 | 178.8 (5) |
C19—N14—C13 | 113.0 (3) | H1L1—O1L—H1L2 | 111.5 |
C15—N14—C13 | 109.8 (3) | H1L1—O1L—H2L1 | 52.4 |
N14—C15—C16 | 108.8 (3) | H1L2—O1L—H2L1 | 135.9 |
N14—C15—H15A | 109.9 | H1L1—O2L—H2L1 | 86.4 |
C16—C15—H15A | 109.9 | H1L1—O2L—H2L2 | 153.9 |
N14—C15—H15B | 109.9 | H2L1—O2L—H2L2 | 102.0 |
C16—C15—H15B | 109.9 | ||
C9—N1—C2—C3 | −0.2 (5) | C12—C13—N14—C19 | −169.0 (3) |
N1—C2—C3—C4 | −0.2 (5) | C12—C13—N14—C15 | 62.3 (4) |
C2—C3—C4—C9 | 0.5 (5) | C19—N14—C15—C16 | 167.6 (4) |
C2—C3—C4—C5 | 174.8 (5) | C13—N14—C15—C16 | −64.4 (4) |
C9—C4—C5—N10 | 174.1 (4) | N14—C15—C16—C17 | 58.3 (5) |
C3—C4—C5—N10 | 0.2 (8) | C15—C16—C17—C18 | −175.4 (4) |
C9—C4—C5—N6 | −3.7 (6) | C15—C16—C17—C12 | −48.6 (5) |
C3—C4—C5—N6 | −177.5 (5) | N10—C12—C17—C18 | 39.5 (5) |
N10—C5—N6—C7 | −175.4 (4) | C13—C12—C17—C18 | 170.1 (4) |
C4—C5—N6—C7 | 2.6 (6) | N10—C12—C17—C16 | −86.7 (4) |
C5—N6—C7—N8 | −0.7 (7) | C13—C12—C17—C16 | 44.0 (5) |
N6—C7—N8—C9 | 0.1 (7) | C15—N14—C19—C20 | −166.0 (4) |
C2—N1—C9—N8 | −179.3 (4) | C13—N14—C19—C20 | 67.7 (5) |
C2—N1—C9—C4 | 0.5 (5) | C15—N14—C19—C23 | 61.8 (5) |
C7—N8—C9—N1 | 178.2 (4) | C13—N14—C19—C23 | −64.6 (5) |
C7—N8—C9—C4 | −1.5 (6) | C15—N14—C19—C22 | −70.7 (5) |
C5—C4—C9—N1 | −176.4 (4) | C13—N14—C19—C22 | 162.9 (3) |
C3—C4—C9—N1 | −0.7 (5) | N14—C19—C20—O21 | 123.8 (4) |
C5—C4—C9—N8 | 3.3 (6) | C23—C19—C20—O21 | −103.5 (4) |
C3—C4—C9—N8 | 179.1 (4) | C22—C19—C20—O21 | 10.2 (3) |
N6—C5—N10—C12 | −1.8 (6) | C19—C20—O21—C22 | −10.7 (3) |
C4—C5—N10—C12 | −179.6 (4) | C20—O21—C22—C19 | 10.6 (3) |
N6—C5—N10—C11 | 178.5 (4) | N14—C19—C22—O21 | −124.0 (4) |
C4—C5—N10—C11 | 0.6 (6) | C20—C19—C22—O21 | −10.2 (3) |
C5—N10—C12—C13 | 125.6 (4) | C23—C19—C22—O21 | 103.2 (4) |
C11—N10—C12—C13 | −54.6 (5) | N14—C19—C23—C24 | 176.8 (4) |
C5—N10—C12—C17 | −105.3 (4) | C20—C19—C23—C24 | 44.4 (5) |
C11—N10—C12—C17 | 74.5 (5) | C22—C19—C23—C24 | −50.7 (5) |
N10—C12—C13—N14 | 79.8 (4) | C19—C23—C24—N25 | −12 (26) |
C17—C12—C13—N14 | −51.0 (5) |