| Bruker SMART APEXII DUO CCD area-detector diffractometer | 10657 independent reflections |
| Radiation source: fine-focus sealed tube | 6269 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.064 |
| φ and ω scans | θmax = 26.5°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −30→32 |
| Tmin = 0.923, Tmax = 0.961 | k = −13→13 |
| 28821 measured reflections | l = −25→25 |