Oxford Diffraction Xcalibur Sapphire3 diffractometer	3576 independent reflections
Radiation source: fine-focus sealed tube	1918 reflections with I > 2σ(I)
Graphite monochromator	Rint = 0.048
Detector resolution: 16.1049 pixels mm-1	θmax = 26.0°, θmin = 3.4°
ω scans	h = −12→10
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2010)	k = −19→19
Tmin = 0.975, Tmax = 0.983	l = −15→15
13349 measured reflections