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31P{1H} NMR spectra of a CD2Cl2 solution of (a) Fe(pdt)(CO)2(dppe) (triangle, unsym isomer; circle, sym isomer), (b) the same solution 30 min after addition of [(acenaphthene)Mn(CO)3]BF4 (diamond, unsym isomer; star, sym isomer), and (c) the same solution after 12 h.
