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. 2014 Apr 7;10:794–807. doi: 10.3762/bjoc.10.75

Table 2.

Parameters of the crystallographic unit cell, measured by X-ray in the B1Rev phase for several compounds at selected temperatures, T.

T / °C a / Å b / Å γ / °

IVb 150 174.2 47.5 91.5
140 200.0 47.8 91.0
130 234.3 48.2 90.8
120 283.8 48.5 91.0
110 370.0 48.8 91.8
Vb 162 142.6 48.2 96.5
150 139.6 48.6 91.9
140 147.6 48.8 90.7
130 158.6 49.1 91.1
120 171.6 49.3 91.4
VIb 126 130.2 48.9 95.9
122 134.4 49.1 95.8
118 140.1 49.3 95.6
114 147.5 49.5 95.1
110 156.1 49.7 94.7
106 166.1 50.0 94.3