Table 1.
Ratio 2a:1a | Conversion of 2a (%) | Yieldsa of 3a, 4a, 5a, % | Overall yieldsa of 3a–5a, % |
1:2 | 100 | 2, 16, 9 | 27 |
1:1.5 | 89 | 5, 22, 17 | 44 |
1:1 | 42 | 19, 37, 15 | 71 |
1.5:1 | 57 | 2, 19, 11 | 32 |
2:1 | 43 | 4, 20, 13 | 37 |
aYield based on consumed azirine 2a.