| Bruker Kappa APEXII diffractometer | 6333 independent reflections |
| Radiation source: fine-focus sealed tube | 4536 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.029 |
| ω and φ scan | θmax = 29.5°, θmin = 2.4° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −11→11 |
| Tmin = 0.922, Tmax = 0.943 | k = −11→11 |
| 25531 measured reflections | l = −20→22 |