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. 2013 Nov 23;69(Pt 12):o1811. doi: 10.1107/S1600536813031140
O1—C6 1.416 (8) C16B—C17B 1.36 (4)
O1—C10 1.426 (8) O2—H2 0.820
O2—C5 1.445 (11) O3—H3 0.820
O3—C7 1.424 (8) C5—H51 0.970
O4A—C10 1.438 (17) C5—H52 0.970
O4A—C11A 1.409 (18) C6—H6 0.980
O4B—C10 1.477 (19) C7—H7 0.980
O4B—C11B 1.42 (3) C8—H8 0.930
C5—C6 1.499 (10) C9—H9 0.930
C6—C7 1.531 (9) C10—H10A 0.980
C7—C8 1.483 (9) C10—H10B 0.980
C8—C9 1.304 (9) C11A—H11A 0.970
C9—C10 1.449 (9) C11A—H11B 0.970
C11A—C12A 1.499 (19) C11B—H11C 0.970
C11B—C12B 1.49 (3) C11B—H11D 0.970
C12A—C13A 1.388 (18) C13A—H13A 0.930
C12A—C17A 1.36 (3) C13B—H13B 0.930
C12B—C13B 1.38 (3) C14A—H14A 0.930
C12B—C17B 1.37 (4) C14B—H14B 0.930
C13A—C14A 1.38 (3) C15A—H15A 0.930
C13B—C14B 1.38 (4) C15B—H15B 0.930
C14A—C15A 1.38 (3) C16A—H16A 0.930
C14B—C15B 1.37 (4) C16B—H16B 0.930
C15A—C16A 1.37 (3) C17A—H17A 0.930
C15B—C16B 1.39 (3) C17B—H17B 0.930
C16A—C17A 1.38 (3)
C6—O1—C10 110.5 (5) C7—C6—H6 108.989
C10—O4A—C11A 111.4 (12) O3—C7—H7 108.061
C10—O4B—C11B 118.8 (16) C6—C7—H7 108.071
O2—C5—C6 109.1 (7) C8—C7—H7 108.069
O1—C6—C5 106.0 (6) C7—C8—H8 118.624
O1—C6—C7 109.3 (5) C9—C8—H8 118.631
C5—C6—C7 114.5 (6) C8—C9—H9 118.863
O3—C7—C6 113.1 (5) C10—C9—H9 118.877
O3—C7—C8 109.9 (6) O1—C10—H10A 108.127
C6—C7—C8 109.5 (5) O1—C10—H10B 112.184
C7—C8—C9 122.7 (6) O4A—C10—H10A 108.127
C8—C9—C10 122.3 (6) O4B—C10—H10B 112.183
O1—C10—O4A 117.6 (7) C9—C10—H10A 108.128
O1—C10—O4B 92.3 (7) C9—C10—H10B 112.184
O1—C10—C9 111.1 (5) O4A—C11A—H11A 109.342
O4A—C10—C9 103.3 (8) O4A—C11A—H11B 109.349
O4B—C10—C9 115.4 (9) C12A—C11A—H11A 109.342
O4A—C11A—C12A 111.4 (11) C12A—C11A—H11B 109.335
O4B—C11B—C12B 110.7 (18) H11A—C11A—H11B 107.980
C11A—C12A—C13A 117.0 (12) O4B—C11B—H11C 109.503
C11A—C12A—C17A 123.9 (12) O4B—C11B—H11D 109.498
C13A—C12A—C17A 119.1 (14) C12B—C11B—H11C 109.496
C11B—C12B—C13B 121.7 (19) C12B—C11B—H11D 109.495
C11B—C12B—C17B 119 (2) H11C—C11B—H11D 108.069
C13B—C12B—C17B 119 (2) C12A—C13A—H13A 119.650
C12A—C13A—C14A 120.7 (13) C14A—C13A—H13A 119.655
C12B—C13B—C14B 120 (2) C12B—C13B—H13B 120.088
C13A—C14A—C15A 117.1 (15) C14B—C13B—H13B 120.082
C13B—C14B—C15B 120 (3) C13A—C14A—H14A 121.432
C14A—C15A—C16A 124.1 (18) C15A—C14A—H14A 121.427
C14B—C15B—C16B 120 (3) C13B—C14B—H14B 119.853
C15A—C16A—C17A 116.3 (15) C15B—C14B—H14B 119.850
C15B—C16B—C17B 119 (2) C14A—C15A—H15A 117.945
C12A—C17A—C16A 122.6 (15) C16A—C15A—H15A 117.953
C12B—C17B—C16B 122 (3) C14B—C15B—H15B 120.031
C5—O2—H2 109.474 C16B—C15B—H15B 120.027
C7—O3—H3 109.475 C15A—C16A—H16A 121.839
O2—C5—H51 109.847 C17A—C16A—H16A 121.842
O2—C5—H52 109.853 C15B—C16B—H16B 120.433
C6—C5—H51 109.854 C17B—C16B—H16B 120.424
C6—C5—H52 109.864 C12A—C17A—H17A 118.712
H51—C5—H52 108.286 C16A—C17A—H17A 118.718
O1—C6—H6 108.978 C12B—C17B—H17B 119.115
C5—C6—H6 108.981 C16B—C17B—H17B 119.099
C6—O1—C10—O4A −173.3 (5) C8—C9—C10—O4A 147.8 (7)
C6—O1—C10—O4B −173.0 (4) C8—C9—C10—O4B 124.1 (7)
C6—O1—C10—C9 −54.6 (6) O4A—C11A—C12A—C13A −68.8 (15)
C10—O1—C6—C5 −168.0 (4) O4A—C11A—C12A—C17A 109.9 (13)
C10—O1—C6—C7 68.1 (5) O4B—C11B—C12B—C13B −111.9 (19)
C10—O4A—C11A—C12A 139.3 (9) O4B—C11B—C12B—C17B 70 (2)
C11A—O4A—C10—O1 −74.9 (11) C11A—C12A—C13A—C14A 179.4 (11)
C11A—O4A—C10—O4B −75.6 (14) C11A—C12A—C17A—C16A 179.8 (12)
C11A—O4A—C10—C9 162.3 (9) C13A—C12A—C17A—C16A −2 (3)
C10—O4B—C11B—C12B −160.8 (10) C17A—C12A—C13A—C14A 1 (2)
C11B—O4B—C10—O1 −58.0 (13) C11B—C12B—C13B—C14B 178.8 (17)
C11B—O4B—C10—O4A 121 (3) C11B—C12B—C17B—C16B −177.4 (19)
C11B—O4B—C10—C9 −172.7 (11) C13B—C12B—C17B—C16B 4 (4)
O2—C5—C6—O1 −176.5 (5) C17B—C12B—C13B—C14B −3 (4)
O2—C5—C6—C7 −56.0 (7) C12A—C13A—C14A—C15A 2 (3)
O1—C6—C7—O3 77.9 (6) C12B—C13B—C14B—C15B 1 (4)
O1—C6—C7—C8 −45.0 (6) C13A—C14A—C15A—C16A −3 (3)
C5—C6—C7—O3 −40.7 (8) C13B—C14B—C15B—C16B −1 (5)
C5—C6—C7—C8 −163.7 (5) C14A—C15A—C16A—C17A 3 (3)
O3—C7—C8—C9 −111.7 (7) C14B—C15B—C16B—C17B 2 (4)
C6—C7—C8—C9 13.0 (9) C15A—C16A—C17A—C12A −0 (3)
C7—C8—C9—C10 −1.1 (11) C15B—C16B—C17B—C12B −4 (4)
C8—C9—C10—O1 20.8 (10)