| Rigaku AFC-7R diffractometer | Rint = 0.034 |
| Radiation source: Rigaku rotating Mo anode | θmax = 27.5° |
| Graphite plate monochromator | h = −9→25 |
| ω–2θ scans | k = 0→6 |
| 1713 measured reflections | l = −7→7 |
| 1585 independent reflections | 3 standard reflections every 150 reflections |
| 786 reflections with F2 > 2σ(F2) | intensity decay: 0.8% |
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