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. 2014 Apr 23;4(2):119–128. doi: 10.1007/s13659-014-0015-5

Table 2.

13C NMR spectroscopic data for compounds 16 in acetone-d6 (δ in ppm)

No 1 a 2 c 3 a 4 b 5 a 6 c
1 118.3, C 118.3, C 117.1, C 111.0, C 117.8, C 118.3, C
2 138.9, C 138.9, C 139.0, C 138.6, C 135.2, C 138.8, C
3 109.4, CH 109.3, CH 109.8, CH 110.1, CH 108.5, CH 109.3, CH
4 156.5, C 156.5, C 157.1, C 157.1, C 158.4, C 156.5, C
5 101.0, CH 101.0, CH 102.2, CH 102.0, CH 95.2, CH 101.0, CH
6 156.4, C 156.4, C 157.9, C 154.7, C 161.6, C 156.4, C
7 19.9, CH3 19.9, CH3 20.5, CH3 19.3, CH3 19.0, CH3 19.9, CH3
8 25.1, CH2 25.1, CH2 34.4, CH2 29.7, CH2 29.1, CH2 25.1, CH2
9 124.8, CH 124.8, CH 77.0, CH 68.4, CH 89.8, CH 124.4, CH
10 134.1, C 134.1, C 153.4, C 78.6, C 73.3, C 134.6, C
11 40.4, CH2 40.4, CH2 32.5, CH2 38.7, CH2 39.3, CH2 37.8, CH2
12 27.2, CH2 27.2, CH2 27.3, CH2 22.1, CH2 22.5, CH2 30.2, CH2
13 124.8, CH 124.8, CH 125.1, CH 125.4, CH 125.6, CH 77.8, CH
14 135.5, C 135.8, C 135.7, C 135.4, C 135.3, C 74.2, C
15 36.4, CH2 37.6, CH2 40.4, CH2 40.4, CH2 40.4, CH2 38.5, CH2
16 34.5, CH2 30.7, CH2 27.3, CH2 27.4, CH2 27.3, CH2 22.6, CH2
17 75.3, CH 78.5, CH 125.1, CH 125.1, CH 125.1, CH 126.2, CH
18 149.3, C 72.9, C 131.6, C 131.6, C 131.6, C 131.1, C
19 17.8, CH3 25.8, CH3 17.7, CH3 17.7, CH3 17.7, CH3 17.6, CH3
20 110.3, CH2 25.8, CH3 25.8, CH3 25.8, CH3 25.8, CH3 25.8, CH3
21 16.1, CH3 16.1, CH3 16.1, CH3 16.0, CH3 16.0, CH3 22.8, CH3
22 16.1, CH3 16.1, CH3 108.9, CH2 17.9, CH3 22.3, CH3 16.3, CH3

aMeasured at 100 MHz

bMeasured at 125 MHz

cMeasured at 150 MHz