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Synthesis of amphiphilic polyamide amine-g-polyethylene glycol graft copolymers.
| Entry | PAA | PAA-g-MPEG | |
|---|---|---|---|
|
BAC/phenylethylamine /ethanolamine |
Graft efficiency* |
||
| Feed ratio | Measured ratio* | ||
| PAA(8:2)-PEG2000 | 9/8/2 | 9/8/2 | 93% |
| PAA(7:3)-PEG2000 | 9/7/3 | 9/7/3 | 84% |
| PAA(6:4)-PEG2000 | 9/6/4 | 9/6/4 | 71% |
| PAA(8:2)-PEG5000 | 9/8/2 | 9/8/2 | 79% |
| PAA(7:3)-PEG5000 | 9/7/3 | 9/7/3 | 67% |
| PAA(6:4)-PEG5000 | 9/6/4 | 9/6/4 | 58% |
*Calculated from peak areas of respective protons in 1H NMR.
