Bruker–Nonius KappaCCD diffractometer | 3099 independent reflections |
Radiation source: sealed X-ray tube | 2333 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.034 |
profile data from φ scans and ω scans | θmax = 25.4°, θmin = 3.3° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −20→20 |
Tmin = 0.932, Tmax = 0.976 | k = −7→6 |
44120 measured reflections | l = −21→21 |