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. 2014 Apr 30;70(Pt 5):o622–o623. doi: 10.1107/S1600536814008204
Bruker–Nonius KappaCCD diffractometer 3099 independent reflections
Radiation source: sealed X-ray tube 2333 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.034
profile data from φ scans and ω scans θmax = 25.4°, θmin = 3.3°
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) h = −20→20
Tmin = 0.932, Tmax = 0.976 k = −7→6
44120 measured reflections l = −21→21