| Bruker X8 Proteum diffractometer | 2501 independent reflections |
| Radiation source: Bruker MicroStar microfocus rotating anode | 2314 reflections with I > 2σ(I) |
| Helios multilayer optics monochromator | Rint = 0.041 |
| Detector resolution: 18.4 pixels mm-1 | θmax = 64.5°, θmin = 4.0° |
| φ and ω scans | h = −10→10 |
| Absorption correction: multi-scan (SADABS; Bruker, 2013) | k = −3→8 |
| Tmin = 0.619, Tmax = 0.643 | l = −25→25 |
| 9744 measured reflections |