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. 2014 Apr 16;70(Pt 5):o560. doi: 10.1107/S1600536814007879
Bruker X8 Proteum diffractometer 2501 independent reflections
Radiation source: Bruker MicroStar microfocus rotating anode 2314 reflections with I > 2σ(I)
Helios multilayer optics monochromator Rint = 0.041
Detector resolution: 18.4 pixels mm-1 θmax = 64.5°, θmin = 4.0°
φ and ω scans h = −10→10
Absorption correction: multi-scan (SADABS; Bruker, 2013) k = −3→8
Tmin = 0.619, Tmax = 0.643 l = −25→25
9744 measured reflections