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. 2014 Apr 17;70(Pt 5):650–655. doi: 10.1107/S2053230X14007171

Table 1. X-ray data-collection statistics for N-acetylmannosamine-6-phosphate 2-epimerase from methicillin-resistant S. aureus .

Values in parentheses are for the highest resolution shell. The Matthews coefficient and solvent content are based on two monomers, with a combined molecular weight of 49 090 Da, in the asymmetric unit.

Wavelength (Å) 0.9537
No. of images 360
Oscillation range (°) 0.5
Space group P21212
Unit-cell parameters (Å, °) a = 77.1, b = 173.7, c = 44.4, α = β = γ = 90
Resolution (Å) 46.3–1.84 (1.88–1.84)
Observed reflections 189024 (9200)
Unique reflections 52704 (3125)
Completeness (%) 99.8 (98.5)
R merge 0.082 (0.549)
R r.i.m. 0.112 (0.738)
R p.i.m. § 0.076 (0.490)
Mean I/σ(I) 10.8 (1.8)
Multiplicity 3.6 (2.9)
Wilson B value (Å2) 9.6
Molecules in asymmetric unit 2
V M3 Da−1) 3.04
Solvent content (%) 59.5

R merge = Inline graphic Inline graphic.

R r.i.m. = Inline graphic Inline graphic.

§

R p.i.m. = Inline graphic Inline graphic, where Ii(hkl) is the ith intensity measurement of reflection hkl, 〈I(hkl)〉 is its average and N(hkl) is the redundancy of a given reflection.