Table 1. X-ray data-collection statistics for N-acetylmannosamine-6-phosphate 2-epimerase from methicillin-resistant S. aureus .
Wavelength (Å) | 0.9537 |
No. of images | 360 |
Oscillation range (°) | 0.5 |
Space group | P21212 |
Unit-cell parameters (Å, °) | a = 77.1, b = 173.7, c = 44.4, α = β = γ = 90 |
Resolution (Å) | 46.3–1.84 (1.88–1.84) |
Observed reflections | 189024 (9200) |
Unique reflections | 52704 (3125) |
Completeness (%) | 99.8 (98.5) |
R merge † | 0.082 (0.549) |
R r.i.m. ‡ | 0.112 (0.738) |
R p.i.m. § | 0.076 (0.490) |
Mean I/σ(I) | 10.8 (1.8) |
Multiplicity | 3.6 (2.9) |
Wilson B value (Å2) | 9.6 |
Molecules in asymmetric unit | 2 |
V M (Å3 Da−1) | 3.04 |
Solvent content (%) | 59.5 |
R merge = .
R r.i.m. = .
R p.i.m. = , where Ii(hkl) is the ith intensity measurement of reflection hkl, 〈I(hkl)〉 is its average and N(hkl) is the redundancy of a given reflection.