Table 1. Fortification experiment of organophosphate pesticides residues from spiked mango at different levels (recovery and repeatability), limit of detection (LOD), limit of quantification (LOQ), maximum residues limits (MRL) and acceptable daily intake (ADI).
| P Pesticides | Fortification level (mg kg−1) | Recovered | (%) Recovery (n = 3) | LOD (mg kg−1) | LOQ (mg kg−1) | %RSDa | MRLb (mg kg−1) | ADIc (mg kg−1day−1) |
| Dichlorvos | 0.05 | 0.039±3.22 | 78.90 | |||||
| 0.10 | 0.080±3.22 | 80.23 | 0.003 | 0.010 | 4.42 | 0.1 | 0.004 | |
| 0.50 | 0.423±3.22 | 84.57 | ||||||
| Phorate | 0.05 | 0.036±3.22 | 72.33 | |||||
| 0.10 | 0.075±3.22 | 75.45 | 0.002 | 0.007 | 3.17 | 0.05 | 0.0005 | |
| 0.50 | 0.391±3.22 | 78.20 | ||||||
| Phorate Sulfone | 0.05 | 0.035±3.22 | 70.22 | |||||
| 0.10 | 0.071±3.22 | 71.45 | 0.010 | 0.033 | 3.84 | 0.05 | 0.0005 | |
| 0.50 | 0.373±3.22 | 74.60 | ||||||
| Phorate Sulfoxide | 0.05 | 0.040±3.22 | 80.35 | |||||
| 0.10 | 0.080±3.22 | 80.00 | 0.003 | 0.010 | 5.35 | 0.05 | 0.0005 | |
| 0.50 | 0.426±3.22 | 85.25 | ||||||
| Dimethoate | 0.05 | 0.039±3.22 | 78.23 | |||||
| 0.10 | 0.080±3.22 | 80.45 | 0.003 | 0.010 | 6.95 | 2.0 | 0.002 | |
| 0.50 | 0.425±3.22 | 85.10 | ||||||
| Diazinon | 0.05 | 0.043±3.22 | 85.28 | |||||
| 0.10 | 0.086±3.22 | 86.30 | 0.001 | 0.004 | 9.50 | NA | 0.02 | |
| 0.50 | 0.450±3.22 | 90.00 | ||||||
| m-Parathion | 0.05 | 0.045±3.22 | 91.11 | |||||
| 0.10 | 0.088±3.22 | 88.35 | 0.001 | 0.004 | 3.23 | 0.2 | 0.003 | |
| 0.50 | 0.467±3.22 | 93.45 | ||||||
| Chlorpyrifos-m | 0.05 | 0.043±3.22 | 85.25 | |||||
| 0.10 | 0.084±3.22 | 83.70 | 0.003 | 0.010 | 4.91 | NA | 0.01 | |
| 0.50 | 0.444±3.22 | 88.90 | ||||||
| Fenitrothion | 0.05 | 0.036±3.22 | 72.90 | |||||
| 0.10 | 0.070±3.22 | 70.20 | 0.010 | 0.033 | 5.37 | 0.5 | 0.005 | |
| 0.50 | 0.372±3.22 | 74.50 | ||||||
| Malathion | 0.05 | 0.041±3.22 | 81.25 | |||||
| 0.10 | 0.082±3.22 | 82.50 | 0.002 | 0.008 | 8.49 | 4.0 | 0.02 | |
| 0.50 | 0.428±3.22 | 85.55 | ||||||
| Chlorpyrifos | 0.05 | 0.045±3.22 | 90.57 | |||||
| 0.10 | 0.092±3.22 | 92.40 | 0.001 | 0.004 | 6.70 | 0.5 | 0.01 | |
| 0.50 | 0.476±3.22 | 95.25 | ||||||
| Chlorfenvinfos | 0.05 | 0.044±3.22 | 88.10 | |||||
| 0.10 | 0.091±3.22 | 90.75 | 0.003 | 0.010 | 6.48 | NA | NA | |
| 0.50 | 0.466±3.22 | 93.25 | ||||||
| Profenofos | 0.05 | 0.042±3.22 | 83.25 | |||||
| 0.10 | 0.080±3.22 | 80.25 | 0.004 | 0.013 | 8.68 | NA | NA | |
| 0.50 | 0.417±3.22 | 83.45 | ||||||
| Ethion | 0.05 | 0.040±3.22 | 80.25 | |||||
| 0.10 | 0.080±3.22 | 80.40 | 0.005 | 0.017 | 8.23 | 2.0 | NA | |
| 0.50 | 0.428±3.22 | 85.70 | ||||||
| Edifenophos | 0.05 | 0.046±3.22 | 92.34 | |||||
| 0.10 | 0.090±3.22 | 90.40 | 0.001 | 0.005 | 7.23 | NA | NA | |
| 0.50 | 0.467±3.22 | 93.50 | ||||||
| Anilophos | 0.05 | 0.039±3.22 | 77.72 | |||||
| 0.10 | 0.079±3.22 | 79.45 | 0.002 | 0.007 | 8.18 | NA | NA | |
| 0.50 | 0.416±3.22 | 83.20 | ||||||
| Phosalone | 0.05 | 0.042±3.22 | 84.22 | |||||
| 0.10 | 0.080±3.22 | 80.50 | 0.003 | 0.010 | 9.61 | 5.0 | 0.02 | |
| 0.50 | 0.431±3.22 | 86.25 |