Table 3.
Screening of the peroxide for the conversion of 1 to 2a
| entry | peroxide | yield(%) |
|---|---|---|
| 1 | TBHP | 88 |
| 2 | CHP | 72 |
| 3 | Bz2O2 | 0 |
| 4 | H2O2 | 0 |
Conditions: substrate (0.1 mmol); NaSO2CF3 (3 equiv); peroxide (5 equiv); TPGS-750-M:Water (2 wt. %).
Screening of the peroxide for the conversion of 1 to 2a
| entry | peroxide | yield(%) |
|---|---|---|
| 1 | TBHP | 88 |
| 2 | CHP | 72 |
| 3 | Bz2O2 | 0 |
| 4 | H2O2 | 0 |
Conditions: substrate (0.1 mmol); NaSO2CF3 (3 equiv); peroxide (5 equiv); TPGS-750-M:Water (2 wt. %).