Table 5.
Direct comparisons with literature 22 examples
| |||||
|---|---|---|---|---|---|
| This Worka | Previous Work | ||||
|
| |||||
| entry | compound |
yield (%)b |
time
(h) |
yield (%)b |
time (h) |
| 1 | 3 | 73 | 43 | 43c | 40 |
| 2 | 4 | 64 | 44 | 51 | 18 |
| 3 | 5 | 62 | 28 | 57 | 24 |
| 4 | 6 | 84 | 23 | 78 | 40 |
| 5 | 7 | 55 | 44 | 48c | 40 |
| 6 | 8 | 54 | 51 | 50c | 40 |
| 7 | 9 | 43 | 38 | 33c | 48 |
| 8 | 10 | 47 | 52 | 43 | 61 |
Conditions: substrate (1 mmol); NaSO2CF3 (3 equiv); TBHP (5 equiv); TPGS-750-M:water (2 wt. %),
See ref. 20. cRequired second addition of reagents.